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# Part of the Crystallography Open Database
# All data on this site have been placed in the public domain by the
# contributors.
#------------------------------------------------------------------------------
#$Date: 2010-06-10 15:11:07 +0000 (Thu, 10 Jun 2010) $
#$Revision: 1210 $
#$URL: svn://cod.ibt.lt/cod/cif/9/9004097.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the American Mineralogist Crystal Structure Database,
# http://rruff.geo.arizona.edu/AMS/amcsd.php
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_9004097
loop_
_publ_author_name
'Hawthorne, F. C.'
'Ferguson, R. B.'
_publ_section_title
;
 Refinement of the crystal structure of cryolite
;
_journal_name_full               'The Canadian Mineralogist'
_journal_page_first              377
_journal_page_last               382
_journal_volume                  13
_journal_year                    1975
_chemical_formula_sum            'Al F6 Na3'
_chemical_name_mineral           Cryolite
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 90.278
_cell_angle_gamma                90
_cell_length_a                   5.4024
_cell_length_b                   5.5959
_cell_length_c                   7.7564
_cell_volume                     234.483
_exptl_crystal_density_diffrn    2.973
_[local]_cod_chemical_formula_sum_orig 'Al Na3 F6'
_cod_database_code               9004097
_amcsd_database_code             AMCSD#0005078
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
1/2+x,1/2-y,1/2+z
1/2-x,1/2+y,1/2-z
-x,-y,-z
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Al 0.00825 0.00827 0.00872 0.00000 0.00004 0.00000
Na1 0.01359 0.01356 0.01365 0.00000 -0.00053 0.00000
Na2 0.01825 0.01767 0.02310 -0.00268 0.00004 0.00033
F1 0.01931 0.02023 0.01033 0.00055 -0.00344 -0.00169
F2 0.01382 0.01731 0.01972 0.00671 0.00376 0.00183
F3 0.01684 0.01344 0.02246 -0.00513 -0.00134 0.00526
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Al 0.00000 0.00000 0.00000
Na1 0.00000 0.00000 0.50000
Na2 0.51330 -0.05190 0.24740
F1 0.10260 0.04550 0.21940
F2 -0.27320 0.17370 0.04620
F3 0.16340 0.26900 -0.06300